ATR microreactor: A tool for in-situ and spatial reaction monitoring

K. Srivastava; N. D. Boyle; K. F.A. Jorissen; I. J. Burgess; W. Van Der Stam; A. Van Den Berg; M. Odijk

doi:10.1109/SENSORS52175.2022.9967095

ATR microreactor: A tool for in-situ and spatial reaction monitoring

K. Srivastava^*
, N. D. Boyle
, K. F.A. Jorissen
, I. J. Burgess
, W. Van Der Stam
, A. Van Den Berg
, M. Odijk

^*Corresponding author for this work

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › Academic › peer-review

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Abstract

We report the fabrication of a microreactor with embedded internal reflection element (IRE) and herringbone (HB) micromixer. The microreactor can be used as a powerful tool for monitoring in-situ chemical reactions when combined with attenuated total internal reflection (ATR) infrared (IR) spectroscopy. In this work, a H2O/D2O model reaction was monitored as a proof of concept and the HOD product formation was spatially tracked. In addition to this, a mixing efficiency of 99% at 25 cycles was also calculated for the microreactor.

Original language	English
Title of host publication	2022 IEEE Sensors, SENSORS 2022 - Conference Proceedings
Publisher	IEEE
Number of pages	4
ISBN (Electronic)	978-1-6654-8464-0
ISBN (Print)	978-1-6654-8465-7
DOIs	https://doi.org/10.1109/SENSORS52175.2022.9967095
Publication status	Published - 8 Dec 2022
Event	2022 IEEE Sensors Conference, SENSORS 2022 - Dallas, United States Duration: 30 Oct 2022 → 2 Nov 2022

Publication series

Name	Proceedings of IEEE Sensors
Volume	2022-October
ISSN (Print)	1930-0395
ISSN (Electronic)	2168-9229

Conference

Conference	2022 IEEE Sensors Conference, SENSORS 2022
Country/Territory	United States
City	Dallas
Period	30/10/22 → 2/11/22

UN SDGs

This output contributes to the following UN Sustainable Development Goals (SDGs)

SDG 9 Industry, Innovation, and Infrastructure

Keywords

insitu reaction monitoring
microreactor
mixers
nanofabrication
2023 OA procedure

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10.1109/SENSORS52175.2022.9967095

ATR_microreactor_A_tool_for_in-situ_and_spatial_reaction_monitoringFinal published version, 601 KBLicence: Taverne

Cite this

@inproceedings{f9fed2b0710a41a193e3f1c9b0c7ecad,

title = "ATR microreactor: A tool for in-situ and spatial reaction monitoring",

abstract = "We report the fabrication of a microreactor with embedded internal reflection element (IRE) and herringbone (HB) micromixer. The microreactor can be used as a powerful tool for monitoring in-situ chemical reactions when combined with attenuated total internal reflection (ATR) infrared (IR) spectroscopy. In this work, a H2O/D2O model reaction was monitored as a proof of concept and the HOD product formation was spatially tracked. In addition to this, a mixing efficiency of 99\% at 25 cycles was also calculated for the microreactor.",

keywords = "insitu reaction monitoring, microreactor, mixers, nanofabrication, 2023 OA procedure",

author = "K. Srivastava and Boyle, \{N. D.\} and Jorissen, \{K. F.A.\} and Burgess, \{I. J.\} and \{Van Der Stam\}, W. and \{Van Den Berg\}, A. and M. Odijk",

note = "Funding Information: We would like to thank the Netherlands Center for Multiscale Catalytic Energy Conversion (MCEC) for funding this project (Grant No. 801359). We would also like to thank the Canadian Light Source (CLS), a research facility of the University of Saskatchewan, for their synchrotron beam facilities. Publisher Copyright: {\textcopyright} 2022 IEEE.; 2022 IEEE Sensors Conference, SENSORS 2022 ; Conference date: 30-10-2022 Through 02-11-2022",

year = "2022",

month = dec,

day = "8",

doi = "10.1109/SENSORS52175.2022.9967095",

language = "English",

isbn = "978-1-6654-8465-7",

series = "Proceedings of IEEE Sensors",

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booktitle = "2022 IEEE Sensors, SENSORS 2022 - Conference Proceedings",

address = "United States",

}

Srivastava, K, Boyle, ND, Jorissen, KFA, Burgess, IJ, Van Der Stam, W, Van Den Berg, A & Odijk, M 2022, ATR microreactor: A tool for in-situ and spatial reaction monitoring. in 2022 IEEE Sensors, SENSORS 2022 - Conference Proceedings. Proceedings of IEEE Sensors, vol. 2022-October, IEEE, 2022 IEEE Sensors Conference, SENSORS 2022, Dallas, Texas, United States, 30/10/22. https://doi.org/10.1109/SENSORS52175.2022.9967095

TY - GEN

T1 - ATR microreactor

T2 - 2022 IEEE Sensors Conference, SENSORS 2022

AU - Srivastava, K.

AU - Boyle, N. D.

AU - Jorissen, K. F.A.

AU - Burgess, I. J.

AU - Van Der Stam, W.

AU - Van Den Berg, A.

AU - Odijk, M.

N1 - Funding Information: We would like to thank the Netherlands Center for Multiscale Catalytic Energy Conversion (MCEC) for funding this project (Grant No. 801359). We would also like to thank the Canadian Light Source (CLS), a research facility of the University of Saskatchewan, for their synchrotron beam facilities. Publisher Copyright: © 2022 IEEE.

PY - 2022/12/8

Y1 - 2022/12/8

N2 - We report the fabrication of a microreactor with embedded internal reflection element (IRE) and herringbone (HB) micromixer. The microreactor can be used as a powerful tool for monitoring in-situ chemical reactions when combined with attenuated total internal reflection (ATR) infrared (IR) spectroscopy. In this work, a H2O/D2O model reaction was monitored as a proof of concept and the HOD product formation was spatially tracked. In addition to this, a mixing efficiency of 99% at 25 cycles was also calculated for the microreactor.

AB - We report the fabrication of a microreactor with embedded internal reflection element (IRE) and herringbone (HB) micromixer. The microreactor can be used as a powerful tool for monitoring in-situ chemical reactions when combined with attenuated total internal reflection (ATR) infrared (IR) spectroscopy. In this work, a H2O/D2O model reaction was monitored as a proof of concept and the HOD product formation was spatially tracked. In addition to this, a mixing efficiency of 99% at 25 cycles was also calculated for the microreactor.

KW - insitu reaction monitoring

KW - microreactor

KW - mixers

KW - nanofabrication

KW - 2023 OA procedure

UR - https://www.scopus.com/pages/publications/85144020350

U2 - 10.1109/SENSORS52175.2022.9967095

DO - 10.1109/SENSORS52175.2022.9967095

M3 - Conference contribution

AN - SCOPUS:85144020350

SN - 978-1-6654-8465-7

T3 - Proceedings of IEEE Sensors

BT - 2022 IEEE Sensors, SENSORS 2022 - Conference Proceedings

PB - IEEE

Y2 - 30 October 2022 through 2 November 2022

ER -

ATR microreactor: A tool for in-situ and spatial reaction monitoring

Abstract

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UN SDGs

Keywords

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