Emulsion compression and coalescence under enhanced gravity studied with in-situ microscopy

T. Krebs*, J.J. Slot, C. P.G.H. Schroen, H.W.M. Hoeijmakers, R.M. Boom

*Corresponding author for this work

    Research output: Chapter in Book/Report/Conference proceedingConference contributionAcademicpeer-review

    1 Citation (Scopus)
    100 Downloads (Pure)

    Abstract

    We report the results of experiments and numerical calculations of compression and coalescence in a monodisperse oil-in-water emulsion upon centrifugation. A custom-built setup allows in-situ monitoring of a rotating bilayer of emulsion droplets using an optical microscope. The oil volume fraction in a compressed layer of oil droplets stabilized against coalescence was measured experimentally as a function of time for different radial accelerations. The sedimentation was simulated using CFD in order to test the applicability of the computationalmethod and the Ishii-Zuber drag law for very high dispersed phase volume fractions. Quantitative agreement of emulsion sedimentation as a function of time between the experiments and simulations is good at higher accelerations, but decreases with decreasing accelerations. Coalescence in a centrifuged emulsion, which was destabilized prior to centrifugation by adding sodium chloride, was also quantified. The growth of a pure oil phase on top of the droplet layer was measured as a function of time. From the growth rate, a characteristic time for droplet coalescence with the pure oil phase was deduced. The experimental method may serve as a tool to study the compression and coalescence kinetics of emulsions under enhanced gravity, which may be of use to assess emulsion stability for industrial applications. Possible improvements of the current experimental setup are also discussed.

    Original languageEnglish
    Title of host publicationAdvances in Fluid Mechanics IX
    EditorsM. Rahman, C.A. Brebbia
    PublisherWIT Press
    Pages199-210
    Number of pages12
    ISBN (Print)9781845646004
    DOIs
    Publication statusPublished - 31 Oct 2012
    Event9th International Conference on Advances in Fluid Mechanics, AFM 2012 - Split, Croatia
    Duration: 26 Jun 201228 Jun 2012
    Conference number: 9

    Publication series

    NameWIT Transactions on Engineering Sciences
    PublisherWIT Press
    Volume74
    ISSN (Print)1743-3533

    Conference

    Conference9th International Conference on Advances in Fluid Mechanics, AFM 2012
    Abbreviated titleAFM IX
    CountryCroatia
    CitySplit
    Period26/06/1228/06/12

    Keywords

    • CFD
    • Coalescence
    • Compression
    • Drag law
    • Droplet
    • Emulsion
    • Microscopy

    Fingerprint Dive into the research topics of 'Emulsion compression and coalescence under enhanced gravity studied with in-situ microscopy'. Together they form a unique fingerprint.

  • Cite this

    Krebs, T., Slot, J. J., Schroen, C. P. G. H., Hoeijmakers, H. W. M., & Boom, R. M. (2012). Emulsion compression and coalescence under enhanced gravity studied with in-situ microscopy. In M. Rahman, & C. A. Brebbia (Eds.), Advances in Fluid Mechanics IX (pp. 199-210). (WIT Transactions on Engineering Sciences; Vol. 74). WIT Press. https://doi.org/10.2495/AFM120181