N,N'-Tetramethylenedibenzamide (TMDB)

Sybolt Harkema, G.J. van Hummel, R.J. Gaymans

Research output: Contribution to journalArticleAcademic

27 Downloads (Pure)

Abstract

Cl8H20N202, monoclinic, P21/c, a = 5.118(3), b = 5.324(3), c = 28.410 (5) /~, B = 97.05 (5)°, Z = 2. The crystal structure was solved by direct methods. All H atoms have been located. R w = 4.7%. The planes of the phenyl ring and the amide group are rotated with respect to each other due to steric hindrance. Hydrogen bonds connect molecules related by translation in the a direction.
Original languageUndefined
Pages (from-to)3182-3184
JournalActa Crystallographica Section B: Structural crystallography and crystal chemistry
Volume36
Issue number12
DOIs
Publication statusPublished - 1980

Keywords

  • IR-59222

Cite this

Harkema, Sybolt ; van Hummel, G.J. ; Gaymans, R.J. / N,N'-Tetramethylenedibenzamide (TMDB). In: Acta Crystallographica Section B: Structural crystallography and crystal chemistry. 1980 ; Vol. 36, No. 12. pp. 3182-3184.
@article{7ced7898e56e48b7b9de464870983361,
title = "N,N'-Tetramethylenedibenzamide (TMDB)",
abstract = "Cl8H20N202, monoclinic, P21/c, a = 5.118(3), b = 5.324(3), c = 28.410 (5) /~, B = 97.05 (5)°, Z = 2. The crystal structure was solved by direct methods. All H atoms have been located. R w = 4.7{\%}. The planes of the phenyl ring and the amide group are rotated with respect to each other due to steric hindrance. Hydrogen bonds connect molecules related by translation in the a direction.",
keywords = "IR-59222",
author = "Sybolt Harkema and {van Hummel}, G.J. and R.J. Gaymans",
year = "1980",
doi = "10.1107/S0567740880011235",
language = "Undefined",
volume = "36",
pages = "3182--3184",
journal = "Acta Crystallographica Section B: Structural crystallography and crystal chemistry",
issn = "0567-7408",
publisher = "Munksgaard International Publishers",
number = "12",

}

N,N'-Tetramethylenedibenzamide (TMDB). / Harkema, Sybolt; van Hummel, G.J.; Gaymans, R.J.

In: Acta Crystallographica Section B: Structural crystallography and crystal chemistry, Vol. 36, No. 12, 1980, p. 3182-3184.

Research output: Contribution to journalArticleAcademic

TY - JOUR

T1 - N,N'-Tetramethylenedibenzamide (TMDB)

AU - Harkema, Sybolt

AU - van Hummel, G.J.

AU - Gaymans, R.J.

PY - 1980

Y1 - 1980

N2 - Cl8H20N202, monoclinic, P21/c, a = 5.118(3), b = 5.324(3), c = 28.410 (5) /~, B = 97.05 (5)°, Z = 2. The crystal structure was solved by direct methods. All H atoms have been located. R w = 4.7%. The planes of the phenyl ring and the amide group are rotated with respect to each other due to steric hindrance. Hydrogen bonds connect molecules related by translation in the a direction.

AB - Cl8H20N202, monoclinic, P21/c, a = 5.118(3), b = 5.324(3), c = 28.410 (5) /~, B = 97.05 (5)°, Z = 2. The crystal structure was solved by direct methods. All H atoms have been located. R w = 4.7%. The planes of the phenyl ring and the amide group are rotated with respect to each other due to steric hindrance. Hydrogen bonds connect molecules related by translation in the a direction.

KW - IR-59222

U2 - 10.1107/S0567740880011235

DO - 10.1107/S0567740880011235

M3 - Article

VL - 36

SP - 3182

EP - 3184

JO - Acta Crystallographica Section B: Structural crystallography and crystal chemistry

JF - Acta Crystallographica Section B: Structural crystallography and crystal chemistry

SN - 0567-7408

IS - 12

ER -