Size distribution of embryos produced by crystal-rod contacts

A.E.D.M. van der Heijden; M. Elwenspoek; J.P. van der Eerden

doi:10.1016/0022-0248(89)90157-7

Size distribution of embryos produced by crystal-rod contacts

A.E.D.M. van der Heijden, M. Elwenspoek, J.P. van der Eerden

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Abstract

We performed contact nucleation experiments on the (010) face of potassium hydrogen phthalate (KAP) crystals growing in a stagnant supersaturated aqueous solution and determined - after a given growth time t - (ex situ) the crystal size distribution (CSD) of the secondary nuclei (which at t = 0 are called "embryos") by using a scanning electron microscope (SEM). The origin of the secondary nuclei could clearly be revealed (damage to the crystal surface). The CSD can be fitted with a log-normal distribution which is typical for many powders obtained by grinding. Minimum size and mean size can be quantitatively understood by elementary fracture mechanics.

Original language	English
Pages (from-to)	398-410
Journal	Journal of crystal growth
Volume	98
Issue number	3
DOIs	https://doi.org/10.1016/0022-0248(89)90157-7
Publication status	Published - 1989

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title = "Size distribution of embryos produced by crystal-rod contacts",

abstract = "We performed contact nucleation experiments on the (010) face of potassium hydrogen phthalate (KAP) crystals growing in a stagnant supersaturated aqueous solution and determined - after a given growth time t - (ex situ) the crystal size distribution (CSD) of the secondary nuclei (which at t = 0 are called {"}embryos{"}) by using a scanning electron microscope (SEM). The origin of the secondary nuclei could clearly be revealed (damage to the crystal surface). The CSD can be fitted with a log-normal distribution which is typical for many powders obtained by grinding. Minimum size and mean size can be quantitatively understood by elementary fracture mechanics.",

author = "{van der Heijden}, A.E.D.M. and M. Elwenspoek and {van der Eerden}, J.P.",

year = "1989",

doi = "10.1016/0022-0248(89)90157-7",

language = "English",

volume = "98",

pages = "398--410",

journal = "Journal of crystal growth",

issn = "0022-0248",

publisher = "Elsevier",

number = "3",

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TY - JOUR

T1 - Size distribution of embryos produced by crystal-rod contacts

AU - van der Heijden, A.E.D.M.

AU - Elwenspoek, M.

AU - van der Eerden, J.P.

PY - 1989

Y1 - 1989

N2 - We performed contact nucleation experiments on the (010) face of potassium hydrogen phthalate (KAP) crystals growing in a stagnant supersaturated aqueous solution and determined - after a given growth time t - (ex situ) the crystal size distribution (CSD) of the secondary nuclei (which at t = 0 are called "embryos") by using a scanning electron microscope (SEM). The origin of the secondary nuclei could clearly be revealed (damage to the crystal surface). The CSD can be fitted with a log-normal distribution which is typical for many powders obtained by grinding. Minimum size and mean size can be quantitatively understood by elementary fracture mechanics.

AB - We performed contact nucleation experiments on the (010) face of potassium hydrogen phthalate (KAP) crystals growing in a stagnant supersaturated aqueous solution and determined - after a given growth time t - (ex situ) the crystal size distribution (CSD) of the secondary nuclei (which at t = 0 are called "embryos") by using a scanning electron microscope (SEM). The origin of the secondary nuclei could clearly be revealed (damage to the crystal surface). The CSD can be fitted with a log-normal distribution which is typical for many powders obtained by grinding. Minimum size and mean size can be quantitatively understood by elementary fracture mechanics.

U2 - 10.1016/0022-0248(89)90157-7

DO - 10.1016/0022-0248(89)90157-7

M3 - Article

VL - 98

SP - 398

EP - 410

JO - Journal of crystal growth

JF - Journal of crystal growth

SN - 0022-0248

IS - 3

ER -