Structure and charge distribution of oxamide as determined from high-order X-ray data

G. de With, Sybolt Harkema

    Research output: Contribution to journalArticleAcademic

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    Abstract

    The crystal structure and electronic charge distribution of oxamide (oxalic acid diamide, C2N202H4) have been determined at 293 K by X-ray methods. The structural results of Ayerst & Duke [Acta Cryst. (1954), 7, 588-590] have been confirmed. High-order data [up to (sin 0)/2 = 1.15 A -~] were collected. A clear indication of bonding features is obtained. The effect of data cut-off on the difference density map has been investigated.
    Original languageUndefined
    Pages (from-to)2367-2372
    JournalActa Crystallographica Section B: Structural crystallography and crystal chemistry
    Volume33
    Issue number8
    DOIs
    Publication statusPublished - 1977

    Keywords

    • IR-59114

    Cite this

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    title = "Structure and charge distribution of oxamide as determined from high-order X-ray data",
    abstract = "The crystal structure and electronic charge distribution of oxamide (oxalic acid diamide, C2N202H4) have been determined at 293 K by X-ray methods. The structural results of Ayerst & Duke [Acta Cryst. (1954), 7, 588-590] have been confirmed. High-order data [up to (sin 0)/2 = 1.15 A -~] were collected. A clear indication of bonding features is obtained. The effect of data cut-off on the difference density map has been investigated.",
    keywords = "IR-59114",
    author = "{de With}, G. and Sybolt Harkema",
    year = "1977",
    doi = "10.1107/S056774087700853X",
    language = "Undefined",
    volume = "33",
    pages = "2367--2372",
    journal = "Acta Crystallographica Section B: Structural crystallography and crystal chemistry",
    issn = "0567-7408",
    publisher = "Munksgaard International Publishers",
    number = "8",

    }

    Structure and charge distribution of oxamide as determined from high-order X-ray data. / de With, G.; Harkema, Sybolt.

    In: Acta Crystallographica Section B: Structural crystallography and crystal chemistry, Vol. 33, No. 8, 1977, p. 2367-2372.

    Research output: Contribution to journalArticleAcademic

    TY - JOUR

    T1 - Structure and charge distribution of oxamide as determined from high-order X-ray data

    AU - de With, G.

    AU - Harkema, Sybolt

    PY - 1977

    Y1 - 1977

    N2 - The crystal structure and electronic charge distribution of oxamide (oxalic acid diamide, C2N202H4) have been determined at 293 K by X-ray methods. The structural results of Ayerst & Duke [Acta Cryst. (1954), 7, 588-590] have been confirmed. High-order data [up to (sin 0)/2 = 1.15 A -~] were collected. A clear indication of bonding features is obtained. The effect of data cut-off on the difference density map has been investigated.

    AB - The crystal structure and electronic charge distribution of oxamide (oxalic acid diamide, C2N202H4) have been determined at 293 K by X-ray methods. The structural results of Ayerst & Duke [Acta Cryst. (1954), 7, 588-590] have been confirmed. High-order data [up to (sin 0)/2 = 1.15 A -~] were collected. A clear indication of bonding features is obtained. The effect of data cut-off on the difference density map has been investigated.

    KW - IR-59114

    U2 - 10.1107/S056774087700853X

    DO - 10.1107/S056774087700853X

    M3 - Article

    VL - 33

    SP - 2367

    EP - 2372

    JO - Acta Crystallographica Section B: Structural crystallography and crystal chemistry

    JF - Acta Crystallographica Section B: Structural crystallography and crystal chemistry

    SN - 0567-7408

    IS - 8

    ER -