Structure and charge distribution of oxamide as determined from high-order X-ray data

G. de With; Sybolt Harkema

doi:10.1107/S056774087700853X

Structure and charge distribution of oxamide as determined from high-order X-ray data

G. de With, Sybolt Harkema

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Abstract

The crystal structure and electronic charge distribution of oxamide (oxalic acid diamide, C2N202H4) have been determined at 293 K by X-ray methods. The structural results of Ayerst & Duke [Acta Cryst. (1954), 7, 588-590] have been confirmed. High-order data [up to (sin 0)/2 = 1.15 A -~] were collected. A clear indication of bonding features is obtained. The effect of data cut-off on the difference density map has been investigated.

Original language	Undefined
Pages (from-to)	2367-2372
Journal	Acta Crystallographica Section B: Structural crystallography and crystal chemistry
Volume	33
Issue number	8
DOIs	https://doi.org/10.1107/S056774087700853X
Publication status	Published - 1977

Keywords

IR-59114

Access to Document

10.1107/S056774087700853X

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Cite this

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title = "Structure and charge distribution of oxamide as determined from high-order X-ray data",

abstract = "The crystal structure and electronic charge distribution of oxamide (oxalic acid diamide, C2N202H4) have been determined at 293 K by X-ray methods. The structural results of Ayerst & Duke [Acta Cryst. (1954), 7, 588-590] have been confirmed. High-order data [up to (sin 0)/2 = 1.15 A -~] were collected. A clear indication of bonding features is obtained. The effect of data cut-off on the difference density map has been investigated.",

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year = "1977",

doi = "10.1107/S056774087700853X",

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journal = "Acta Crystallographica Section B: Structural crystallography and crystal chemistry",

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T1 - Structure and charge distribution of oxamide as determined from high-order X-ray data

AU - de With, G.

AU - Harkema, Sybolt

PY - 1977

Y1 - 1977

N2 - The crystal structure and electronic charge distribution of oxamide (oxalic acid diamide, C2N202H4) have been determined at 293 K by X-ray methods. The structural results of Ayerst & Duke [Acta Cryst. (1954), 7, 588-590] have been confirmed. High-order data [up to (sin 0)/2 = 1.15 A -~] were collected. A clear indication of bonding features is obtained. The effect of data cut-off on the difference density map has been investigated.

AB - The crystal structure and electronic charge distribution of oxamide (oxalic acid diamide, C2N202H4) have been determined at 293 K by X-ray methods. The structural results of Ayerst & Duke [Acta Cryst. (1954), 7, 588-590] have been confirmed. High-order data [up to (sin 0)/2 = 1.15 A -~] were collected. A clear indication of bonding features is obtained. The effect of data cut-off on the difference density map has been investigated.

KW - IR-59114

U2 - 10.1107/S056774087700853X

DO - 10.1107/S056774087700853X

M3 - Article

SN - 0567-7408

VL - 33

SP - 2367

EP - 2372

JO - Acta Crystallographica Section B: Structural crystallography and crystal chemistry

JF - Acta Crystallographica Section B: Structural crystallography and crystal chemistry

IS - 8

ER -