Abstract
A new one-step procedure for the synthesis of monoalkylated calix[4]arenes is presented. Reaction of calix[4]arene 1a or 1b with 1.2 equivalent of a weak base (K2CO3 in MeCN or CsF in DMF) and excess of alkylating agent affords the monoalkylated calix[4]arenes in moderate to good yields
Original language | Undefined |
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Pages (from-to) | 8379-8384 |
Number of pages | 6 |
Journal | Tetrahedron |
Volume | 0 |
Issue number | 47 |
DOIs | |
Publication status | Published - 1991 |
Keywords
- METIS-106725
- IR-12544