Temperature dependent lattice distortion and high temperature phase transition of pseudo-cubic bis(tetramethylammonium) hexafluorotitanate(IV), (TMA)2[TiF6]

Ole Göbel, Johan E. ten Elshof, A.M.M. Schreurs

Research output: Contribution to journalArticleAcademicpeer-review

5 Citations (Scopus)

Abstract

The crystal structure of (TMA)2[TiF6] between –173 °C and 180 °C was refined on the basis of single crystal diffraction data. A phase transition from rhombohedral to cubic at approx. 142 °C was found by measuring the birefringence as a function of temperature, and confirmed by the refined crystal structures
Original languageEnglish
Pages (from-to)748-755
Number of pages9
JournalZeitschrift für Kristallographie
Volume226
Issue number9
DOIs
Publication statusPublished - 2011

Keywords

  • METIS-280145

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