The crystal and molecular structure of 2,7-diazanaphthalene

C. Huiszoon, G.J. van Hummel, D.M.W. van den Ham

Research output: Contribution to journalArticleAcademic

40 Downloads (Pure)

Abstract

X-ray diffraction data were collected at 20°C on a computer-controlled Philips diffractometer (PW 1100). The structure was solved by direct methods and refined by the full-matrix least-squares method to an R of 0.065 (weighted R 0.046). The molecule in the crystal is of lower symmetry than C2,.. The geometry of the molecule has been compared with NMR results obtained by Danieli, Lunazzi & Veracini [J. Chem. Soc. Perkin II, (1976), pp. 19-201. As a result a C-H bond-length correction of 0.09 (2) A was found.
Original languageUndefined
Pages (from-to)1867-1870
JournalActa Crystallographica Section B: Structural crystallography and crystal chemistry
Volume33
DOIs
Publication statusPublished - 1977

Keywords

  • IR-59235

Cite this

Huiszoon, C. ; van Hummel, G.J. ; van den Ham, D.M.W. / The crystal and molecular structure of 2,7-diazanaphthalene. In: Acta Crystallographica Section B: Structural crystallography and crystal chemistry. 1977 ; Vol. 33. pp. 1867-1870.
@article{3e906a7049b24370926d6a17bd3e32c5,
title = "The crystal and molecular structure of 2,7-diazanaphthalene",
abstract = "X-ray diffraction data were collected at 20°C on a computer-controlled Philips diffractometer (PW 1100). The structure was solved by direct methods and refined by the full-matrix least-squares method to an R of 0.065 (weighted R 0.046). The molecule in the crystal is of lower symmetry than C2,.. The geometry of the molecule has been compared with NMR results obtained by Danieli, Lunazzi & Veracini [J. Chem. Soc. Perkin II, (1976), pp. 19-201. As a result a C-H bond-length correction of 0.09 (2) A was found.",
keywords = "IR-59235",
author = "C. Huiszoon and {van Hummel}, G.J. and {van den Ham}, D.M.W.",
year = "1977",
doi = "10.1107/S0567740877007225",
language = "Undefined",
volume = "33",
pages = "1867--1870",
journal = "Acta Crystallographica Section B: Structural crystallography and crystal chemistry",
issn = "0567-7408",
publisher = "Munksgaard International Publishers",

}

The crystal and molecular structure of 2,7-diazanaphthalene. / Huiszoon, C.; van Hummel, G.J.; van den Ham, D.M.W.

In: Acta Crystallographica Section B: Structural crystallography and crystal chemistry, Vol. 33, 1977, p. 1867-1870.

Research output: Contribution to journalArticleAcademic

TY - JOUR

T1 - The crystal and molecular structure of 2,7-diazanaphthalene

AU - Huiszoon, C.

AU - van Hummel, G.J.

AU - van den Ham, D.M.W.

PY - 1977

Y1 - 1977

N2 - X-ray diffraction data were collected at 20°C on a computer-controlled Philips diffractometer (PW 1100). The structure was solved by direct methods and refined by the full-matrix least-squares method to an R of 0.065 (weighted R 0.046). The molecule in the crystal is of lower symmetry than C2,.. The geometry of the molecule has been compared with NMR results obtained by Danieli, Lunazzi & Veracini [J. Chem. Soc. Perkin II, (1976), pp. 19-201. As a result a C-H bond-length correction of 0.09 (2) A was found.

AB - X-ray diffraction data were collected at 20°C on a computer-controlled Philips diffractometer (PW 1100). The structure was solved by direct methods and refined by the full-matrix least-squares method to an R of 0.065 (weighted R 0.046). The molecule in the crystal is of lower symmetry than C2,.. The geometry of the molecule has been compared with NMR results obtained by Danieli, Lunazzi & Veracini [J. Chem. Soc. Perkin II, (1976), pp. 19-201. As a result a C-H bond-length correction of 0.09 (2) A was found.

KW - IR-59235

U2 - 10.1107/S0567740877007225

DO - 10.1107/S0567740877007225

M3 - Article

VL - 33

SP - 1867

EP - 1870

JO - Acta Crystallographica Section B: Structural crystallography and crystal chemistry

JF - Acta Crystallographica Section B: Structural crystallography and crystal chemistry

SN - 0567-7408

ER -