Time-Resolved Small-Angle X-Ray Scattering

Johan E. ten Elshof, R. Besselink, Tomasz Stawski, H.L. Castricum

Research output: Chapter in Book/Report/Conference proceedingChapterAcademicpeer-review

1 Citation (Scopus)

Abstract

This chapter focuses on time-resolved studies of nanostructure development in sol-gel liquids, that is, diluted sols, wet gels, and drying thin fffilms. The most commonly investigated classes of sol-gel materials are silica, organically modified silica, template-directed mesostructured silica, titania and titania-based materials, zirconia and zirconia-based materials, and few others. After a brief overview of small-angle X-ray scattering (SAXS) theory and some experimental details, the chapter discusses separately each of these classes of sol-gel materials. Nearly all time-resolved SAXS studies on silica have been carried out starting with alkoxysilanes. The chapter discusses studies of systems with a single precursor under acidic and basic conditions, respectively, and reviews combinations of alkoxysilanes with other metal precursors and mixed organic-inorganic systems.

Original languageEnglish
Title of host publicationThe Sol-Gel Handbook. Synthesis, Characterization, and Applications
EditorsD. Levy, M. Zayat
Place of PublicationWeinheim
PublisherWiley-VCH Verlag
Pages673-712
Number of pages40
Volume2-3
ISBN (Electronic)9783527670819
ISBN (Print)978-3-527-33486-5
DOIs
Publication statusPublished - 14 Sep 2015

Publication series

NameChapter 21
PublisherWiley VCH

Fingerprint

X ray scattering
Silicon Dioxide
Silica
Sol-gels
Zirconia
Titanium
Time and motion study
Polymethyl Methacrylate
Sols
Nanostructures
Drying
Gels
Metals
Liquids
titanium dioxide
zirconium oxide

Keywords

  • Mesostructured silica
  • Organically modified silica
  • SAXS experiments
  • Sol-gel systems
  • Time-resolved small-angle X-ray scattering
  • Time-resolved studies
  • Titanates
  • Zirconates

Cite this

ten Elshof, J. E., Besselink, R., Stawski, T., & Castricum, H. L. (2015). Time-Resolved Small-Angle X-Ray Scattering. In D. Levy, & M. Zayat (Eds.), The Sol-Gel Handbook. Synthesis, Characterization, and Applications (Vol. 2-3, pp. 673-712). (Chapter 21). Weinheim: Wiley-VCH Verlag. https://doi.org/10.1002/9783527670819.ch21
ten Elshof, Johan E. ; Besselink, R. ; Stawski, Tomasz ; Castricum, H.L. / Time-Resolved Small-Angle X-Ray Scattering. The Sol-Gel Handbook. Synthesis, Characterization, and Applications. editor / D. Levy ; M. Zayat. Vol. 2-3 Weinheim : Wiley-VCH Verlag, 2015. pp. 673-712 (Chapter 21).
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ten Elshof, JE, Besselink, R, Stawski, T & Castricum, HL 2015, Time-Resolved Small-Angle X-Ray Scattering. in D Levy & M Zayat (eds), The Sol-Gel Handbook. Synthesis, Characterization, and Applications. vol. 2-3, Chapter 21, Wiley-VCH Verlag, Weinheim, pp. 673-712. https://doi.org/10.1002/9783527670819.ch21

Time-Resolved Small-Angle X-Ray Scattering. / ten Elshof, Johan E.; Besselink, R.; Stawski, Tomasz; Castricum, H.L.

The Sol-Gel Handbook. Synthesis, Characterization, and Applications. ed. / D. Levy; M. Zayat. Vol. 2-3 Weinheim : Wiley-VCH Verlag, 2015. p. 673-712 (Chapter 21).

Research output: Chapter in Book/Report/Conference proceedingChapterAcademicpeer-review

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ten Elshof JE, Besselink R, Stawski T, Castricum HL. Time-Resolved Small-Angle X-Ray Scattering. In Levy D, Zayat M, editors, The Sol-Gel Handbook. Synthesis, Characterization, and Applications. Vol. 2-3. Weinheim: Wiley-VCH Verlag. 2015. p. 673-712. (Chapter 21). https://doi.org/10.1002/9783527670819.ch21